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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1406022Generated: October 31, 2026

Hydrochloric Acid → HCID 86701837, compound

https://huagongshe.com/reaction/1406022

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 60151776HCID 60151776—
SolventMethanolHCID 887—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 86701837HCID 86701837—

Reaction Steps

To a solution of N-(2,6-diethylphenyl)-9-{[2-methoxy-4-(4-methylpiperazin-1-yl)phenyl]amino}-1-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl]-1,4,5,6-tetrahydropyrazolo[4′,3′:6,7]cyclohepta[1,2-d]pyrimidine-3-carboxamide (0.040 g, 0.056 mmol) in MeOH (0.6 mL), 4M HCl in dioxane (0.010 mL) was added. The mixture was stirred at room temperature for 1 h. The organic solvent was evaporated to dryness to give the title compound in quantitative yield.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08916577B2
Source datasetuspto-grants-2014_12
ORD IDord-67650075068f4a9c8c5867ee5552dc66
Source noteuspto-grants-2014_12