HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86701837, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 60151776 | HCID 60151776 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 86701837 | HCID 86701837 | — |
Reaction Steps
To a solution of N-(2,6-diethylphenyl)-9-{[2-methoxy-4-(4-methylpiperazin-1-yl)phenyl]amino}-1-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl]-1,4,5,6-tetrahydropyrazolo[4′,3′:6,7]cyclohepta[1,2-d]pyrimidine-3-carboxamide (0.040 g, 0.056 mmol) in MeOH (0.6 mL), 4M HCl in dioxane (0.010 mL) was added. The mixture was stirred at room temperature for 1 h. The organic solvent was evaporated to dryness to give the title compound in quantitative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08916577B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-67650075068f4a9c8c5867ee5552dc66 |
| Source note | uspto-grants-2014_12 |