HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxylamine → 4-(4-Bromo-2-chloro-phenoxy)-benzaldehyde-oxime
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | 4-(4-Bromo-2-chloro-phenoxy)-benzaldehyde | HCID 28893153 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 4-(4-Bromo-2-chloro-phenoxy)-benzaldehyde-oxime | HCID 86658818 | — |
Reaction Steps
20 mg (0.06 mmol) of 4-(4-bromo-2-chloro-phenoxy)-benzaldehyde were stirred with 20 μL (0.33 mmol) of hydroxylamine solution (50% in water) in 2 mL f DMF at 80° C. for 1 h. The reaction mixture was purified by chromatography (reversed phase).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08916589B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-64fa39e5ed964d61b5f7065c943dcdbc |
| Source note | uspto-grants-2014_12 |