Dimethylformamide → HCID 21250395, compound

HRID 1406444Notes

Reaction equation

HRID 1406444 reaction equation
[NH2:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](O)=[O:7])=[CH:4][C:3]=1[N+:11]([O-:13])=[O:12].S(Cl)([Cl:16])=O.CN(C=O)C>ClCCl>[NH2:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([Cl:16])=[O:7])=[CH:4][C:3]=1[N+:11]([O-:13])=[O:12]

Participants

5

Reactant 3

HCID 6228DimethylformamideHCID 24386Thionyl ChlorideHCID 74115Benzoic acid, 4-amino-3-nitro-

Product 1

HCID 21250395HCID 21250395, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Prepared analogously to example 53a from 4-amino-3-nitro-benzoic acid with thionyl chloride and DMF in dichloromethane at reflux.

Workup

  1. temperatureat reflux

Sources & evidence

ORD record
ord-9e8f35c37fe4461698e919f35d01d9c9
Source dataset
uspto-grants-2014_12
Patent number
US08916599B2

Reaction notes

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