Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | HCID 69594216 | HCID 69594216 | — |
| Product | HCID 45089373 | HCID 45089373 | — |
Reaction Steps
A mixture of 4-acteylamino-2-methyl-3-nitro-benzoic acid (4.8 g, 20.2 mmol) and 6 M HCl (aq) (150 mL) in 120 mL dioxane was stirred for 15 min at 105° C. The mixture was cooled, filtered and washed with water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08916599B2 |
|---|
| Source dataset | uspto-grants-2014_12 |
|---|
| ORD ID | ord-f44a97351dd1430f9036c18955a4eccd |
|---|
| Source note | uspto-grants-2014_12 |
|---|
