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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1406497Generated: October 30, 2026

Dicyclohexylcarbodiimide → HCID 67230261, compound

https://huagongshe.com/reaction/1406497

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDicyclohexylcarbodiimideHCID 10868—
Reactant1,3-Dichloro-2-isothiocyanatobenzeneHCID 123239—
ReactantMethyl 3-amino-4-(methylamino)benzoateHCID 15586064—
SolventEthanolHCID 702—
SolventDimethylformamideHCID 6228—
SolventSodium HydroxideHCID 14798—
ProductHCID 67230261HCID 67230261—

Reaction Steps

Prepared analogously to example 113a from 3-amino-4-methylamino-benzoic acid methyl ester and 1,3-dichloro-2-isothiocyanato-benzene with DCC in DMF and NaOH in ethanol.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08916599B2
Source datasetuspto-grants-2014_12
ORD IDord-e8c8e15d41fe4df3bc8fdc4fbb0f94b8
Source noteuspto-grants-2014_12