HCID 7406921, compound → HCID 67230022, compound

HRID 1406506Notes

Reaction equation

HRID 1406506 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:9](=[O:21])[C:10]2[CH:15]=[CH:14][C:13]([NH:16][CH3:17])=[C:12]([N+:18]([O-])=O)[CH:11]=2)=[CH:4][CH:3]=1>C(O)(=O)C.[Fe]>[NH2:18][C:12]1[CH:11]=[C:10]([CH:15]=[CH:14][C:13]=1[NH:16][CH3:17])[C:9]([NH:8][C:5]1[CH:4]=[CH:3][C:2]([Br:1])=[CH:7][CH:6]=1)=[O:21]

Participants

4

Reactant 1

HCID 7406921HCID 7406921, compound

Product 1

HCID 67230022HCID 67230022, compound

Reagents, catalysts & solvents 2

HCID 23925IronCatalystHCID 176Acetic AcidSolvent

Procedure

Prepared analogously to example 91a from N-(4-bromo-phenyl)-4-methylamino-3-nitro-benzamide and iron powder in acetic acid.

Sources & evidence

ORD record
ord-46ba20fc8b504895bffd87edb7f5c7b2
Source dataset
uspto-grants-2014_12
Patent number
US08916599B2

Reaction notes

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