Acetic Acid → HCID 86660392, compound

HRID 1406514Notes

Reaction equation

HRID 1406514 reaction equation
[C:1]([C:3]1[CH:4]=[CH:5][C:6]([NH:9][C:10](=[O:23])[C:11]2[CH:16]=[CH:15][C:14]([N+:17]([O-])=O)=[C:13]([N+:20]([O-])=O)[CH:12]=2)=[N:7][CH:8]=1)#[N:2].C(O)(=O)C>C(O)C.[Fe]>[NH2:20][C:13]1[CH:12]=[C:11]([CH:16]=[CH:15][C:14]=1[NH2:17])[C:10]([NH:9][C:6]1[CH:5]=[CH:4][C:3]([C:1]#[N:2])=[CH:8][N:7]=1)=[O:23]

Participants

5

Reactant 2

HCID 176Acetic AcidHCID 86660391HCID 86660391, compound

Product 1

HCID 86660392HCID 86660392, compound

Reagents, catalysts & solvents 2

HCID 23925IronCatalystHCID 702EthanolSolvent

Procedure

Prepared analogously to example 91a from N-(5-cyano-pyridin-2-yl)-3,4-dinitro-benzamide, iron powder and glacial acetic acid in ethanol.

Sources & evidence

ORD record
ord-ca9585beae8348b9950c8986053fe940
Source dataset
uspto-grants-2014_12
Patent number
US08916599B2

Reaction notes

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