O,O-Dipyridin-2-yl carbonothioate → HCID 86660393, compound

HRID 1406515Notes

Reaction equation

HRID 1406515 reaction equation
[Cl:1][C:2]1[C:3]([C:9]([F:12])([F:11])[F:10])=[C:4]([NH2:8])[CH:5]=[CH:6][CH:7]=1.N1C=CC=CC=1O[C:20](=[S:28])OC1C=CC=CN=1>C1COCC1>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([N:8]=[C:20]=[S:28])[C:3]=1[C:9]([F:10])([F:11])[F:12]

Participants

4

Reactant 2

HCID 719784O,O-Dipyridin-2-yl carbonothioateHCID 137504423-Chloro-2-(trifluoromethyl)aniline

Product 1

HCID 86660393HCID 86660393, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

Prepared analogously to example 192a from 3-chloro-2-trifluoromethyl-phenylamine, thiocarbonic acid O,O-dipyridin-2-yl ester and TEA in THF.

Sources & evidence

ORD record
ord-05d8c1f1b8d045bc8974ebbe65f73b89
Source dataset
uspto-grants-2014_12
Patent number
US08916599B2

Reaction notes

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