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HRID1408442

反应详情

EQUATION

反应方程式

HRID 1408442 的结构方程式

REACTANTS

反应物

2
结构：Clc1nc(N2CCOCC2)nc(N2CCOCC2)n1
HCID224967

2-Chloro-4,6-bis(morpholin-4-yl)-1,3,5-triazine

C11H16ClN5O2

结构：CC1(C)OB(c2ccc(C#N)cc2)OC1(C)C
HCID2734625

4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)benzonitrile

C13H16BNO2

PRODUCTS

生成物

1
结构：N#Cc1ccc(-c2nc(N3CCOCC3)nc(N3CCOCC3)n2)cc1
HCID58507720

未命名化合物

收率 40%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCCC.CCOC(C)=O
溶剂HCID21226206

未命名化合物

PROCEDURE

实验过程

Following the general procedure A, 4,4′-(6-chloro-1,3,5-triazine-2,4-diyl)dimorpholine was coupled with 4-cyanophenylboronic acid pinacol ester with reaction time of 15 h. Chromatography (hexane/ethyl acetate 1:1) gave the 40% of the title compound as a colorless solid.