2-Chloro-4,6-bis(morpholin-4-yl)-1,3,5-triazine → HCID 58507795, compound

Participants

Role	Name	HCID	Charge
Reactant	2-Chloro-4,6-bis(morpholin-4-yl)-1,3,5-triazine	HCID 224967	—
Reactant	4-(5-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-2-pyridinyl)morpholine	HCID 2795363	—
Solvent	Ethyl acetate hexane	HCID 21226206	—
Product	HCID 58507795	HCID 58507795	—

Reaction Steps

Following the general procedure A, 4,4′-(6-chloro-1,3,5-triazine-2,4-diyl)dimorpholine was coupled with 6-(morpholin-4-yl)pyridine-3-boronic acid pinacol ester acid pinacol ester with reaction time of 15 h. Chromatography (hexane/ethyl acetate 1:1) gave the title compound as a colorless solid.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US08921361B2
Source dataset	uspto-grants-2014_12
ORD ID	ord-5aa3f22c0f304fecac2395fd6fb471f8
Source note	uspto-grants-2014_12