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HRID1408445

反应详情

EQUATION

反应方程式

HRID 1408445 的结构方程式

REACTANTS

反应物

2
结构：Clc1nc(N2CCOCC2)nc(N2CCOCC2)n1
HCID224967

2-Chloro-4,6-bis(morpholin-4-yl)-1,3,5-triazine

C11H16ClN5O2

结构：CC1(C)OB(c2cnc(N)cc2C(F)(F)F)OC1(C)C
HCID57416499

5-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-4-(trifluoromethyl)pyridin-2-amine

C12H16BF3N2O2

PRODUCTS

生成物

1
结构：Nc1cc(C(F)(F)F)c(-c2nc(N3CCOCC3)nc(N3CCOCC3)n2)cn1
HCID58507717

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO.ClCCl
溶剂HCID21226129

未命名化合物

PROCEDURE

实验过程

Following the general procedure A, 4,4′-(6-chloro-1,3,5-triazine-2,4-diyl)dimorpholine was coupled with 5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-(trifluoromethyl)pyridin-2-amine with reaction time of 15 h. Chromatography (dichlormethane/methanol 97:3) gave the title compound as an colorless oil.