Cyanuric chloride → HCID 58508124, compound

HRID 1408449Notes

Reaction equation

HRID 1408449 reaction equation
Cl[C:2]1[N:7]=[C:6]([Cl:8])[N:5]=[C:4]([Cl:9])[N:3]=1.[NH2:10][CH2:11][C:12]1[CH:13]=[N:14][CH:15]=[CH:16][CH:17]=1>>[Cl:9][C:4]1[N:5]=[C:6]([Cl:8])[N:7]=[C:2]([NH:10][CH2:11][C:12]2[CH:13]=[N:14][CH:15]=[CH:16][CH:17]=2)[N:3]=1

Participants

3

Reactant 2

HCID 7954Cyanuric chlorideHCID 310183-Pyridinemethanamine

Product 1

HCID 58508124HCID 58508124, compound

Procedure

Following the general procedure A, 2,4,6-trichloro-1,3,5-triazine was coupled with 3-aminomethylpyridine with reaction time of 2 h. Purification by column chromatography gave the title compound.

Workup

  1. customPurification by column chromatography

Sources & evidence

ORD record
ord-b1765f4b8fdb478eaf027b2fa10ef97c
Source dataset
uspto-grants-2014_12
Patent number
US08921361B2

Reaction notes

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