Cyanuric chloride → HCID 58508111, compound

HRID 1408450Notes

Reaction equation

HRID 1408450 reaction equation
Cl[C:2]1[N:7]=[C:6]([Cl:8])[N:5]=[C:4]([Cl:9])[N:3]=1.[NH2:10][CH2:11][C:12]1[CH:17]=[CH:16][N:15]=[CH:14][CH:13]=1>>[Cl:9][C:4]1[N:5]=[C:6]([Cl:8])[N:7]=[C:2]([NH:10][CH2:11][C:12]2[CH:17]=[CH:16][N:15]=[CH:14][CH:13]=2)[N:3]=1

Participants

3

Reactant 2

HCID 7954Cyanuric chlorideHCID 773174-Pyridinemethanamine

Product 1

HCID 58508111HCID 58508111, compound

Procedure

Following the general procedure A, 2,4,6-trichloro-1,3,5-triazine was coupled with 4-aminomethylpyridine with reaction time of 2 h. Purification by column chromatography gave the title compound.

Workup

  1. customPurification by column chromatography

Sources & evidence

ORD record
ord-303059665a064f1e995e22a62fe4201d
Source dataset
uspto-grants-2014_12
Patent number
US08921361B2

Reaction notes

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