Cyanuric chloride → HCID 58508167, compound

HRID 1408451Notes

Reaction equation

HRID 1408451 reaction equation
Cl[C:2]1[N:7]=[C:6]([Cl:8])[N:5]=[C:4]([Cl:9])[N:3]=1.[NH2:10][CH2:11][CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][N:14]=1>>[Cl:9][C:4]1[N:5]=[C:6]([Cl:8])[N:7]=[C:2]([NH:10][CH2:11][CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][N:14]=2)[N:3]=1

Participants

3

Reactant 2

HCID 7954Cyanuric chlorideHCID 759192-Pyridineethanamine

Product 1

HCID 58508167HCID 58508167, compound

Procedure

Following the general procedure A, 2,4,6-trichloro-1,3,5-triazine was coupled with 2-(2-aminoethyl)pyridine with reaction time of 2 h. Purification by column chromatography gave the title compound.

Workup

  1. customPurification by column chromatography

Sources & evidence

ORD record
ord-7f93709bcd6a471d844fc2ea9b899b2b
Source dataset
uspto-grants-2014_12
Patent number
US08921361B2

Reaction notes

Loading…