Cyanuric chloride → HCID 58507703, compound

HRID 1408453Notes

Reaction equation

Cl[C:2]1[N:7]=[C:6]([Cl:8])[N:5]=[C:4]([Cl:9])[N:3]=1.[NH2:10][CH2:11][CH2:12][C:13]1[CH:18]=[CH:17][N:16]=[CH:15][CH:14]=1>>[Cl:9][C:4]1[N:5]=[C:6]([Cl:8])[N:7]=[C:2]([NH:10][CH2:11][CH2:12][C:13]2[CH:18]=[CH:17][N:16]=[CH:15][CH:14]=2)[N:3]=1

Participants

Reactant 2

HCID 7954Cyanuric chloride

HCID 832754-Pyridineethanamine

Product 1

HCID 58507703HCID 58507703, compound

Procedure

Following the general procedure A 2,4,6-trichloro-1,3,5-triazine was coupled with 4-(2-Aminoethyl)pyridine with reaction time of 2 h. Purification by column chromatography gave the title compound.

Workup

customPurification by column chromatography

Sources & evidence

ORD record: ord-2359209471344f4cbeaf146e5fc528fe
Source dataset: uspto-grants-2014_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08921361B2

Reaction notes

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