HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 178481310, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | 3-Pyridinylboronic acid | HCID 2734378 | — |
| Reactant | HCID 178481309 | HCID 178481309 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 178481310 | HCID 178481310 | — |
Reaction Steps
To a solution of 6-bromo-2′-imino-1′-methyl-2-phenyl-2′,3′-dihydro-1′H-spiro[chroman-4,4′-pyrimidin]-6′(5′H)-one TFA salt (12 mg, 0.023 mmol) and pyridin-3-ylboronic acid (9 mg, 0.070 mmol) in 1,4-dioxane (3 mL) charged in a 10-mL microwave test tube is added Cs2CO3 (63 mg, 0.195 mmol) and H2O (0.5 mL), followed by
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08921359B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-8eb7afd876e64f98bbd1c568abc28d91 |
| Source note | uspto-grants-2014_12 |