Tributyltin azide → HCID 178477295, compound

Participants

Reaction Steps

A solution of 6-cyano-4-(ethylthio)pyrrolo[1,2-b]pyridazine-3-carboxamide (140 mg, 0.568 mmol) and azidotributyltin (0.187 mL, 0.682 mmol) in NMP (2.0 mL) was heated to 180° C. for 60 minutes under microwave oven (CEM). The reaction mixture was taken to the next step without purification. MS (ES+) m/z: 290.08 (M+H).

Provenance & Evidence