HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 86714676, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 86714675 | HCID 86714675 | — |
| Product | HCID 86714676 | HCID 86714676 | — |
Reaction Steps
The title compound was prepared using the procedure described in Example 32(d) starting from (S)-ethyl 4-((1-(3-(3-chloro-4-cyano-5-fluorophenyl)-1H-pyrazol-1-yl)propan-2-yl)carbamoyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-imidazole-2-carboxylate (5.22 mmol, 3 g) and sodium hydroxide (7.83 mmol, 313 mg). Yield 1.49 g. LC-MS: [M+1]=547.28.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08921378B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-4f9587943d934f5c9906f94852e4c68e |
| Source note | uspto-grants-2014_12 |