HCID 70980814, compound → HCID 70981983, compound

Participants

Reaction Steps

The title compound was prepared using the procedure described in Example 58(e) starting from the mixture of methyl 2-(1-ethoxyethyl)-1-((2-(trimethylsilyl)-ethoxy)methyl)-1H-imidazole-4-carboxylate and ethyl 2-(1-ethoxyethyl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-imidazole-4-carboxylate (600 mg). Yield 370 mg. 1H-NMR (400 MHz; DMSO-d6): δ −0.01 (s, 9H), 0.86 (t, 2H), 1.08 (d, 3H), 1.45 (t, 3H), 3.41 (q, 2H), 3.50 (t, 2H), 4.71 (q, 1H), 5.42 (s, 2H), 7.92 (s, 1H), 12.13 (bs, 1H). LC-MS: [M+1]=315.12.

Provenance & Evidence