HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 56654141, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 2-(5,6-dihydro-2H-pyran-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane | HCID 15836633 | — |
| Reactant | HCID 86689250 | HCID 86689250 | — |
| Product | HCID 56654141 | HCID 56654141 | — |
Reaction Steps
The title compound was synthesized by procedures and steps analogous to those described in Example 14 above, but using (S)-3-Chloro-1-fluoro-7-(2-fluoropyridin-3-yl)spiro[chromeno[2,3-c]pyridine-5,3′-pyrrolo[3,4-c]pyridin]-1′-amine 2,2,2-trifluoroacetate (14d-2) and 2-(5,6-dihydro-2H-pyran-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in step 5. MS m/z=496.0 [M+H]+. Calculated for: C28H19F2N5O2.O2HF3O2: 609.50 (TFA salt)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08921363B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-6a87ed62172348fe811943f0fbd5fd2c |
| Source note | uspto-grants-2014_12 |