HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzylamine → HCID 136377083, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzylamine | HCID 67326 | — |
| Reactant | HCID 136377081 | HCID 136377081 | — |
| Product | HCID 136377083 | HCID 136377083 | 18% |
Reaction Steps
The synthesis performed as in Example 21 using methyl 2-(biphenyl-2-ylmethyl)-5-hydroxy-6-oxo-1,6-dihydropyrimidine-4-carboxylate (0.070 g, 208 μmol) and 4-fluorobenzylamine (0.5 ml; 4.38 mmol) to provide the title compound as an off-white solid (0.016 g; 18%). LCMS: m/z=430 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08921388B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-333e2d8692bb40a5865196662db917be |
| Source note | uspto-grants-2014_12 |