HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triacetoxyperiodinane → 1-(5-Ethyl-pyrazin-2-yl)-piperidin-4-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triacetoxyperiodinane | HCID 159087 | — |
| Reactant | HCID 67608386 | HCID 67608386 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 1-(5-Ethyl-pyrazin-2-yl)-piperidin-4-one | HCID 68290037 | — |
Reaction Steps
The title compound is prepared from 1-(5-ethyl-pyrazin-2-yl)-piperidin-4-ol by oxidation with Dess-Martin periodinane in dichloromethane at room temperature. LC (method 7): tR=0.73 min; Mass spectrum (ESI+): m/z=206 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08921398B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-5d7195145e374b18957f84173dafc4dd |
| Source note | uspto-grants-2014_12 |