HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methyl-2-butenoic acid → HCID 178447384, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methyl-2-butenoic acid | HCID 10931 | — |
| Reactant | HCID 178478713 | HCID 178478713 | — |
| Product | HCID 178447384 | HCID 178447384 | — |
Reaction Steps
The title compound, off-white solid (83 mg, 81%), MS (ISP) m/z=409.4 [(M+H)+], mp 147° C., was prepared in accordance with the general method of example 1 from trans-4-[2-(4-benzofuran-3-yl-piperidin-1-yl)-ethyl]-cyclohexylamine dihydrochloride (intermediate A) (100 mg, 0.25 mmol) and 3-methyl-but-2-enoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08921397B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-b91bca6de32a4558ae7515e7c706a17e |
| Source note | uspto-grants-2014_12 |