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HRID1409983

反应详情

EQUATION

反应方程式

HRID 1409983 的结构方程式

REACTANTS

反应物

4
结构：Br
HCID260

Hydrogen Bromide

BrH

结构：O=C(CBr)c1cccnc1
HCID151408

3-(2-Bromoacetyl)pyridine

C7H6BrNO

结构：CCOC(=O)c1cc(-c2cccnc2)nn1CC(=O)c1cc(OC)ccc1OC
HCID86267540

未命名化合物

结构：CCOC(=O)c1cc([Si](C)(C)C)n[nH]1
HCID178469409

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1cc([Si](C)(C)C)nn1CC(=O)c1cccnc1
HCID86267746

未命名化合物

PROCEDURE

实验过程

This compound was made in an analogous fashion to ethyl 1-(2-(2,5-dimethoxyphenyl)-2-oxoethyl)-3-(pyridin-3-yl)-1H-pyrazole-5-carboxylate using ethyl 3-(trimethylsilyl)-1H-pyrazole-5-carboxylate and 2-bromo-1-(pyridin-3-yl)ethanone.HBr (purchased from Aldrich). 1H-NMR δ 9.20 (d, 1H), 8.84 (dd, 1H), 8.25 (dt, 1H), 7.46 (dd, 1H), 7.07 (s, 1H), 6.05 (s, 2H), 4.26 (q, 2H), 1.31 (t, 3H), 0.32 (s, 9H). Calculated mass for C16H21N3O3Si, 331.14, observed, 332.0 (M+1).