HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxybenzaldehyde → N-[(2-Methoxyphenyl)methylidene]benzenecarbohydrazonic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxybenzaldehyde | HCID 8658 | — |
| Reactant | Benzoylhydrazine | HCID 11955 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | N-[(2-Methoxyphenyl)methylidene]benzenecarbohydrazonic acid | HCID 287909 | — |
Reaction Steps
A suspension of 1.5 g (7.3 mmol) 2-methoxybenzaldehyde and 1 g (7.3 mmol) benzhydrazide in 35 mL n-hexane was stirred overnight at room temperature. The precipitate was suctioned off, dried, and used without further purification (1.75 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08921406B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-34920d3f5ed3497caf7a08ae7f3ccfe1 |
| Source note | uspto-grants-2014_12 |