2-Methoxybenzaldehyde → N-[(2-Methoxyphenyl)methylidene]benzenecarbohydrazonic acid

HRID 1410182Notes

Reaction equation

HRID 1410182 reaction equation
[CH3:1][O:2][C:3]1[CH:10]=[CH:9][CH:8]=[CH:7][C:4]=1[CH:5]=O.[C:11]([NH:19][NH2:20])(=[O:18])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>CCCCCC>[CH3:1][O:2][C:3]1[CH:10]=[CH:9][CH:8]=[CH:7][C:4]=1[CH:5]=[N:20][NH:19][C:11](=[O:18])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

4

Reactant 2

HCID 86582-MethoxybenzaldehydeHCID 11955Benzoylhydrazine

Product 1

HCID 287909N-[(2-Methoxyphenyl)methylidene]benzenecarbohydrazonic acid

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

A suspension of 1.5 g (7.3 mmol) 2-methoxybenzaldehyde and 1 g (7.3 mmol) benzhydrazide in 35 mL n-hexane was stirred overnight at room temperature. The precipitate was suctioned off, dried, and used without further purification (1.75 g).

Workup

  1. customdried
  2. customused without further purification (1.75 g)

Sources & evidence

ORD record
ord-34920d3f5ed3497caf7a08ae7f3ccfe1
Source dataset
uspto-grants-2014_12
Patent number
US08921406B2

Reaction notes

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