HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Thiocarbonyldi-2(1H)-pyridone → HCID 86646334, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Thiocarbonyldi-2(1H)-pyridone | HCID 853162 | — |
| Reactant | HCID 59529800 | HCID 59529800 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86646334 | HCID 86646334 | — |
Reaction Steps
N-[1-(3-Amino-4-chlorophenyl)ethyl]acetamide (90 mg, 0.2 mmol) was added to a mixture of 1,1′-thiocarbonyldi-2-pyridone (69 mg, 0.2 mmol), DMAP (7 mg, 0.05 mmol) and DCM (2 mL) at rt. The mixture was concentrated and used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08921405B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-3d8ff490b6f8494db2991573d585605c |
| Source note | uspto-grants-2014_12 |