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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1410193Generated: October 28, 2026

HCID 67230022, compound → HCID 59529808, compound

https://huagongshe.com/reaction/1410193

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67230022HCID 67230022—
ReactantHCID 86646334HCID 86646334—
SolventDimethylformamideHCID 6228—
ProductHCID 59529808HCID 59529808—

Reaction Steps

N-[1-(4-Chloro-3-isothiocyanatophenyl)ethyl]acetamide in DMF (2 mL) was added to a mixture of 3-amino-N-(4-bromophenyl)-4-methylaminobenzamide (87 mg, 0.2 mmol, crude material from the step above) in DMF (2 mL) at rt. The mixture was stirred at rt overnight and concentrated. The residue was purified by chromatography to give the sub-title compound. Yield: 130 mg.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08921405B2
Source datasetuspto-grants-2014_12
ORD IDord-61544b6e73ea4961aed7993696c5fdf6
Source noteuspto-grants-2014_12