HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67230022, compound → HCID 59529808, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67230022 | HCID 67230022 | — |
| Reactant | HCID 86646334 | HCID 86646334 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 59529808 | HCID 59529808 | — |
Reaction Steps
N-[1-(4-Chloro-3-isothiocyanatophenyl)ethyl]acetamide in DMF (2 mL) was added to a mixture of 3-amino-N-(4-bromophenyl)-4-methylaminobenzamide (87 mg, 0.2 mmol, crude material from the step above) in DMF (2 mL) at rt. The mixture was stirred at rt overnight and concentrated. The residue was purified by chromatography to give the sub-title compound. Yield: 130 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08921405B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-61544b6e73ea4961aed7993696c5fdf6 |
| Source note | uspto-grants-2014_12 |