HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(2,3-DIHYDRO-1,4-BENZODIOXIN-6-YL)ACRYLIC ACID → HCID 67772854, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(2,3-DIHYDRO-1,4-BENZODIOXIN-6-YL)ACRYLIC ACID | HCID 6173840 | — |
| Reactant | 2-[4-(1H-Indol-3-yl)-cyclohexylamino]-2-piperidin-4-yl-acetamide dihydrochloride | HCID 67775194 | — |
| Product | HCID 67772854 | HCID 67772854 | — |
Reaction Steps
The title compound was prepared from the product of Example 1, step J, and trans-3-(2,3-dihydro-1,4-benzodioxin-7-yl)prop-2-enoic acid, by the method of Example 1, step K, giving a solid that was mostly the more polar cyclohexyl diastereomers by LCMS. Mass spectrum (LCMS, ESI pos.) calcd. for C32H38N4O4: 543 (M+H). Found: 543
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08921559B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-f0deaf86f8af43f29f57188b09cccd66 |
| Source note | uspto-grants-2014_12 |