HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 54204017, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Epibromohydrin | HCID 18430 | — |
| Reactant | HCID 54260250 | HCID 54260250 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 54204017 | HCID 54204017 | — |
Reaction Steps
A mixture of 31 g of 5-cyano-8-hydroxy-1,4-benzodioxane (VII) (Code number 770583), 38.35 g of epibromohydrin and 133 g of potassium carbonate in 300 ml of acetonitrile was brought to reflux for 12 hours. The mixture was filtered, the product then crystallized in the filtrate, it was filtered out and recrystallized in acetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04248788 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-f7393267758e4932bf647a6d2e1a9f1e |
| Source note | uspto-grants-1981_02 |