HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → HCID 53743283, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-(2,3-Dihydro-8-hydroxy-1,4-benzodioxin-5-yl)ethan-1-one | HCID 80337 | — |
| Product | HCID 53743283 | HCID 53743283 | 95% |
Reaction Steps
A suspension of 97 g (0.5 mole) of 5 hydroxy-8-acetyl-1,4-benzodioxane (VIIi), of 127 g (1 mole) of benzyl chloride and 155 g (1.12 mole) of potassium carbonate in 150 ml of absolute alcohol was brought to reflux for 24 hours. After filtration the solvent was evaporated, the residue was taken up in chloroform, washed with a solution of soda (NaOH) 1 N, the solvent was evaporated and the product was crystallized in alcohol, 135 g of product expected were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04248788 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-5bcccd7e9b1e41e79eac8333140f4d50 |
| Source note | uspto-grants-1981_02 |