Morpholine → HCID 20549212, compound

Participants

Reaction Steps

1-Ethyl-2-methylcycloheptanecarbonyl chloride (1.5 g, 0.007 mole) in ether (10 ml.) was added slowly to a solution of morpholine (0.02 mole) in ether (10 ml.). The mixture was washed with dilute hydrochloric acid, dilute sodium bicarbonate and then with water. The ether layer was dried and distilled to give N-(1-ethyl-2-methylcycloheptanecarbonyl) morpholine bp. 145°-7°/0.35 mm.

Provenance & Evidence