Thionyl Chloride → HCID 12797528, compound

HRID 1413129Notes

Reaction equation

HRID 1413129 reaction equation
[C:1]([S:5][CH2:6][CH:7]([CH3:11])[C:8](O)=[O:9])(=[O:4])[CH2:2][CH3:3].S(Cl)([Cl:14])=O>>[C:1]([S:5][CH2:6][CH:7]([CH3:11])[C:8]([Cl:14])=[O:9])(=[O:4])[CH2:2][CH3:3]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 12764104HCID 12764104, compound

Product 1

HCID 12797528HCID 12797528, compound

Procedure

A mixture of 3-propanoylthio-2-methylpropanoic acid (19.7 g) and thionyl chloride (16 g) was stirred at room temperature overnight. The reaction mixture was distilled under reduced pressure to give the title compound, b.p. 135°-137° C. (35 mmHg).

Workup

  1. distillationThe reaction mixture was distilled under reduced pressure

Sources & evidence

ORD record
ord-b9611e2390894e01a1d76dd6ff9316ab
Source dataset
uspto-grants-1981_02
Patent number
US04248883

Reaction notes

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