HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 12797528, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 12764104 | HCID 12764104 | — |
| Product | HCID 12797528 | HCID 12797528 | — |
Reaction Steps
A mixture of 3-propanoylthio-2-methylpropanoic acid (19.7 g) and thionyl chloride (16 g) was stirred at room temperature overnight. The reaction mixture was distilled under reduced pressure to give the title compound, b.p. 135°-137° C. (35 mmHg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04248883 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-b9611e2390894e01a1d76dd6ff9316ab |
| Source note | uspto-grants-1981_02 |