HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → HCID 86737442, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | Triphenylphosphine Oxide | HCID 13097 | — |
| Product | HCID 86737442 | HCID 86737442 | — |
Reaction Steps
In accordance with the invention, triphenylphosphine oxide is reacted with phosgene in chloroform to form a triphenylphosphine dichloride-chloroform adduct. The resulting adduct is reduced with hydrogen to form the desired triphenylphosphine. The reduction may proceed in chloroform as a solvent or in the absence of a solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04249023 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-3094e1c3ae334dd798d8b5ba69b1b57c |
| Source note | uspto-grants-1981_02 |