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HRID1413220

反应详情

EQUATION

反应方程式

HRID 1413220 的结构方程式

REACTANTS

反应物

2
结构：ClC(Cl)Cl.[Cl-].[Cl-].c1ccc(P(c2ccccc2)c2ccccc2)cc1
HCID86737442

未命名化合物

结构：[H][H]
HCID178418361

未命名化合物

PRODUCTS

生成物

1
结构：c1ccc(P(c2ccccc2)c2ccccc2)cc1
HCID11776

Triphenylphosphine

C18H15P

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClC(Cl)Cl
溶剂HCID6212

Chloroform

CHCl3

PROCEDURE

实验过程

reducing said triphenylphosphine dichloride-chloroform adduct with hydrogen at a temperature of at least about 130° C. in the presence of chloroform as the solvent or in the absence of a solvent, to give triphenylphosphine.

WORKUP

后处理

  1. customof at least about 130° C.