Diphenyl Ether → HCID 13548756, compound

HRID 1413286Notes

Reaction equation

HRID 1413286 reaction equation
C[S:2][C:3](=S)[NH:4][N:5]=[CH:6][C:7]1[N:8]=[C:9]([CH3:12])[NH:10][CH:11]=1.C1(OC2C=CC=CC=2)C=CC=CC=1>>[CH3:12][C:9]1[N:8]2[C:3](=[S:2])[NH:4][N:5]=[CH:6][C:7]2=[CH:11][N:10]=1

Participants

3

Reactant 2

HCID 7583Diphenyl EtherHCID 178504098HCID 178504098, compound

Product 1

HCID 13548756HCID 13548756, compound

Procedure

A mixture of 53.9 gm. of 3-(2-methyl-4-imidazolyl-methylene)dithiocarbazic acid methyl ester and 200 ml. of diphenyl ether is reacted as described in Example 58 giving the desired product, m.p. 280.5°-284° C.

Workup

  1. additionA mixture of 53.9 gm

Sources & evidence

ORD record
ord-8b701a528c4840739e1d13e0205cae8a
Source dataset
uspto-grants-1981_02
Patent number
USRE030511

Reaction notes

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