Diphenyl Ether → HCID 13548680, compound

HRID 1413290Notes

Reaction equation

C([O:3][C:4](=O)[NH:5][N:6]=[CH:7][C:8]1[N:9]=[C:10]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[NH:11][CH:12]=1)C.C1(OC2C=CC=CC=2)C=CC=CC=1>>[C:13]1([C:10]2[N:9]3[C:4](=[O:3])[NH:5][N:6]=[CH:7][C:8]3=[CH:12][N:11]=2)[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

Participants

Reactant 2

HCID 7583Diphenyl Ether

HCID 178473578HCID 178473578, compound

Product 1

HCID 13548680HCID 13548680, compound

Procedure

A 7.76 gm. portion of 3-(2-phenyl-4-imidazolylmethylene)carbazic acid ethyl ester in 50 ml. of diphenyl ether is reacted as described in Example 70 giving the desired product m.p. 245°-248° C.

Sources & evidence

ORD record: ord-c1c0e99b7cf0486888886ca29c0e69a8
Source dataset: uspto-grants-1981_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: USRE030511

Reaction notes

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