Diphenyl Ether → HCID 13548684, compound
Reaction equation
C([O:3][C:4](=O)[NH:5][N:6]=[CH:7][C:8]1[N:9]=[C:10]([CH3:13])[NH:11][CH:12]=1)C.C1(OC2C=CC=CC=2)C=CC=CC=1>>[CH3:13][C:10]1[N:9]2[C:4](=[O:3])[NH:5][N:6]=[CH:7][C:8]2=[CH:12][N:11]=1Participants
3
Procedure
A 27.2 gm. portion of 3-(2-methyl-4-imidazolylmethylene)carbazic acid ethyl ester in 200 ml. of diphenyl ether is reacted as described in Example 70 giving the desired product m.p. 303°-305.5° C.
Sources & evidence
- ORD record
- ord-8cf4511c09804b4b8bdbd17b46237268
- Source dataset
- uspto-grants-1981_02
- Patent number
- USRE030511
Reaction notes
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