HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → HCID 20291497, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | Methyl 3-azabicyclo[3.1.0]hexane-2-carboxylate | HCID 20060492 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20291497 | HCID 20291497 | 70% |
Reaction Steps
By a method analogous to that of Example 1, this compound was prepared from 2-methoxycarbonyl-3-azabicyclo(3.1.0)hexane. Sodium dissolved in methanol instead of ethanol was used as dehydrohalogenating agent. The desired compound was obtained as a straw-colored liquid in 70% yield. Its identity was confirmed by elemental analysis, and by NMR and IR analyses.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04249936 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-2ef7b3e230ff478098242edcbad0d9f5 |
| Source note | uspto-grants-1981_02 |