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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1413316Generated: November 2, 2026

O-Allylhydroxylamine → HCID 178460154, compound

https://huagongshe.com/reaction/1413316

Reaction equation

Participants

RoleNameHCIDCharge
ReactantO-AllylhydroxylamineHCID 420841—
ReactantHCID 20291509HCID 20291509—
SolventEthanolHCID 702—
ProductHCID 178460154HCID 17846015467.6%

Reaction Steps

6 g of 2-butyryl-5-(2-ethylsulfinylpropyl)-cyclohexane-1,3-dione was dissolved in 30 ml of ethanol. To the solution was added 1.6 g of allyloxyamine and the resulting solution was stirred at room temperature for 15 hours. After completion of the reaction, the reaction solution was treated as in Example 1 to obtain 4.8 g of the desired compound as colorless oily material.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04249937
Source datasetuspto-grants-1981_02
ORD IDord-966c489c6edb4d61806134dae5b8467b
Source noteuspto-grants-1981_02