HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Allylhydroxylamine → HCID 178460154, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Allylhydroxylamine | HCID 420841 | — |
| Reactant | HCID 20291509 | HCID 20291509 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178460154 | HCID 178460154 | 67.6% |
Reaction Steps
6 g of 2-butyryl-5-(2-ethylsulfinylpropyl)-cyclohexane-1,3-dione was dissolved in 30 ml of ethanol. To the solution was added 1.6 g of allyloxyamine and the resulting solution was stirred at room temperature for 15 hours. After completion of the reaction, the reaction solution was treated as in Example 1 to obtain 4.8 g of the desired compound as colorless oily material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04249937 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-966c489c6edb4d61806134dae5b8467b |
| Source note | uspto-grants-1981_02 |