Hydroxylamine, O-ethyl- → HCID 178474725, compound

Participants

Reaction Steps

1.6 g of 2-propionyl-5-[2-(4-chlorophenylthio)ethyl]cyclohexane-1,3-dione was allowed to react with 0.8 g of ethoxyamine at room temperature for 16 hours in 60 ml of methanol. After completion of the reaction, the resulting reaction solution was treated as in Example 1 to obtain oily product. Purification of the oily product by column chromatography gave 1 g of the desired compound as colorless oily material.

Provenance & Evidence