HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 178474722, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | O-Allylhydroxylamine | HCID 420841 | — |
| Reactant | HCID 20291505 | HCID 20291505 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178474722 | HCID 178474722 | 68.1% |
Reaction Steps
1.3 g of 2-propionyl-5-[1-(p-tolylthio)isopropyl]cyclohexane-1,3-dione was allowed to react with 0.3 g of allyloxyamine at room temperature for 15 hours in the mixture of 10 ml of benzene and 3 ml of ethanol. After completion of the reaction, the resulting reaction solution was treated as in Example 1 to obtain 1 g of the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04249937 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-9e7b91a6e4f645edaa38669c88e490a8 |
| Source note | uspto-grants-1981_02 |