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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1413319Generated: November 4, 2026

Benzene → HCID 178474722, compound

https://huagongshe.com/reaction/1413319

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzeneHCID 241—
ReactantO-AllylhydroxylamineHCID 420841—
ReactantHCID 20291505HCID 20291505—
SolventEthanolHCID 702—
ProductHCID 178474722HCID 17847472268.1%

Reaction Steps

1.3 g of 2-propionyl-5-[1-(p-tolylthio)isopropyl]cyclohexane-1,3-dione was allowed to react with 0.3 g of allyloxyamine at room temperature for 15 hours in the mixture of 10 ml of benzene and 3 ml of ethanol. After completion of the reaction, the resulting reaction solution was treated as in Example 1 to obtain 1 g of the desired compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04249937
Source datasetuspto-grants-1981_02
ORD IDord-9e7b91a6e4f645edaa38669c88e490a8
Source noteuspto-grants-1981_02