HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 20291458, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Butanoic acid, 4-chloro-4-oxo-, methyl ester | HCID 73888 | — |
| Reactant | HCID 20291461 | HCID 20291461 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 20291458 | HCID 20291458 | — |
Reaction Steps
To 19.3 milliliters of 25 percent w/v, 2-phenyl-5-methoxymethyl oxazolidine solution in 50 milliliters of benzene with 3.8 grams of 3-carbomethoxyproprionyl chloride was added 2.0 grams of 50% sodium hydroxide. After the reaction was complete the mixture was washed with water, separated, dried and the organic solvent removed in vacuo. There was obtained 6.8 grams of the title compound, nD30 1.4913. Analytical data supports the structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04249931 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-785123b5cc8746baaa160eb999dd281d |
| Source note | uspto-grants-1981_02 |