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HRID1413332

反应详情

EQUATION

反应方程式

HRID 1413332 的结构方程式

REACTANTS

反应物

2
结构：Nc1cccc(S(=O)(=O)O)c1
HCID8474

3-Aminobenzenesulfonic acid

C6H7NO3S

结构：N#CSCC(=O)c1ccccc1
HCID219693

Phenacyl thiocyanate

C9H7NOS

PRODUCTS

生成物

1
结构：O=S(=O)(O)c1cccc(Nc2nc(-c3ccccc3)cs2)c1
HCID20291805

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Cl-].[Cl-].[Zn+2]
催化剂HCID3007855

Zinc chloride

Cl2Zn

结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

132 parts of phenacyl thiocyanate, 38 parts of zinc chloride and 129 parts of 1-aminobenzene-3-sulfonic acid are together stirred with 750 parts of water for 20 hours at the boil. After the mixture has cooled, the product is filtered off and dried.

WORKUP

后处理

  1. temperatureAfter the mixture has cooled
  2. filtrationthe product is filtered off
  3. customdried