HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromoacetyl bromide → HCID 20291819, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromoacetyl bromide | HCID 61147 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | HCID 20291821 | HCID 20291821 | — |
| Product | HCID 20291819 | HCID 20291819 | — |
Reaction Steps
In the manner given in Preparation 2, 7,9-dimethyl-5-[p-(methylthio)phenyl]-3H-1,4-benzodiazepin-2-yl hydrazine was reacted with bromoacetyl bromide and after 1.5 hours with sodium acetate, than the mixture was refluxed to give 8,10-dimethyl-1-(bromomethyl)-6-[p-(methylthio)phenyl]-4H-s-triazolo[4,3-a][1,4]benzodiazepine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04250094 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-244bab1c77d24dbeb3959f4f5893eeeb |
| Source note | uspto-grants-1981_02 |