HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 20290839, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 12751641 | HCID 12751641 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20290839 | HCID 20290839 | 101.9% |
Reaction Steps
To a solution of 94.1 g (0.43 mole) of 2-(4-fluorophenyl)-1-(2-thienyl)ethanone in 700 ml. of ether was added dropwise a solution of 65.0 g. (0.41 mole of bromine in 140 ml. of methylene chloride at room temperature with stirring. The solvent was removed under vacuum to give 125.0 g of 2-bromo-2-(4-fluorophenyl)-1-(2-thienyl)ethanone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04251535 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-65b951d330014c6e8325b1556d6c3dde |
| Source note | uspto-grants-1981_02 |