HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butylamine → 3-Isopropyl-5-[2-(2-hydroxy-3-tert.-butylaminopropoxy)-styryl]-isoxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butylamine | HCID 6385 | — |
| Reactant | 3-Isopropyl-5-[2-(2,3-epoxypropoxy)-styryl]-isoxazole | HCID 54459054 | — |
| Product | 3-Isopropyl-5-[2-(2-hydroxy-3-tert.-butylaminopropoxy)-styryl]-isoxazole | HCID 56633979 | — |
Reaction Steps
7 g (0.025 mole) of 3-isopropyl-5-[2-(2,3-epoxypropoxy)-styryl]-isoxazole and 3.6 g (0.05 mole) of tert.-butylamine are reacted by the method described in Example 4. 5.8 g (59% of theory) of colorless crystals are obtained. Melting point 191°-193° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04251539 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-bed7e878abab43dc9134aba95af53974 |
| Source note | uspto-grants-1981_02 |