HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butylamine → 3-tert.-Butyl-5-[2-(2-hydroxy-3-tert.-butylaminopropoxy)-styryl]-isoxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butylamine | HCID 6385 | — |
| Reactant | 3-Tert.-butyl-5-[2-(2,3-epoxypropoxy)-styryl]-isoxazole | HCID 56628877 | — |
| Product | 3-tert.-Butyl-5-[2-(2-hydroxy-3-tert.-butylaminopropoxy)-styryl]-isoxazole | HCID 56625385 | — |
Reaction Steps
7 g (0.023 mole) of 3-tert.-butyl-5-[2-(2,3-epoxypropoxy)-styryl]-isoxazole and 3.4 g (0.047 mole) of tert.-butylamine are reacted by the method described in Example 4. 6.8 g (72% of theory) of colorless crystals are obtained. Melting point 207°-208° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04251539 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-20713af56de94e78a653061e3e8e0492 |
| Source note | uspto-grants-1981_02 |