HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → barium bis(nonylphenolate)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | 4-Nonylphenol | HCID 1752 | — |
| Reactant | Barium | HCID 5355457 | — |
| Reactant | Barium Oxide Nanoparticle Dispersion | HCID 9855530 | — |
| Solvent | 1-Octanol | HCID 957 | — |
| Solvent | Water | HCID 962 | — |
| Product | barium bis(nonylphenolate) | HCID 14029936 | — |
Reaction Steps
Nonylphenol 110 g (0.5 mole), toluene 80 g, octanol 20 g and barium oxide 115 g (0.75 mole) were stirred and treated with 13.5 g water. Reaction proceeded with exothermic heat, and was continued nder reflux for 1 hour. After cooling, the mixture was filtered and there was obtained a black-green liquid overbased barium nonylphenolate complex, which was analyzed to find barium: 28% metal ratio:6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04252698 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-dd22d70c304d44fbadcd774c399558e1 |
| Source note | uspto-grants-1981_02 |